Ball milling: a green technology for the preparation and functionalisation of nanocellulose derivatives. Carmen C. Piras a, Susana Fernández-Prieto b and Wim M. De Borggraeve * a a Molecular Design and Synthesis, Department of Chemistry, KU Leuven – University of Leuven, Celestijnenlaan 200F, Box 2404, B-3001 Leuven, Belgium...The ball milling was performed in 1 h intervals with 30 min interval breaks at 300 rpm. The jars of the samples that were ball milled under a nitrogen atmosphere were purged with nitrogen for 1 min before milling. The different samples were ball milled for a total milling time of 1 h, 2 h, 4 h, 8 h, 12 h, 18 h and 24 h.

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